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KMID : 0370219960400020131
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Yakhak Hoeji
1996 Volume.40 No. 2 p.131 ~ p.134
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Synthesis of Xylopinine
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황순호/Hwang SH
김남재/홍유화/김인종/김신규/Kim NJ/Hong YH/Kim IJ/Kim SK
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Abstract
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3,4-Dimethoxyphenethyl amine(1) and 3,4-dimethoxybenzaldehyde were converted to compounds(4) through sucessive condensation and reduction reaction. Compound(4) was treated with methylthioacetyl chloride to give compound(5) then m-chloroperbenzoic acid(m-CPBA) treatment of compound(5) produced S-oxide(6). To obtain isoquinoline derivative(7),(8), compound(6) were treated with p-TsOH. Xylopinine(9) and it’’s derivatives(10) were produced by Bischler-Napieralski reaction.
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KEYWORD
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